4-Butylaniline → HCID 53704978、化合物

反応式

[CH2:1]([C:5]1[CH:11]=[CH:10][C:8]([NH2:9])=[CH:7][CH:6]=1)[CH2:2][CH2:3][CH3:4].C1(C2C=CC(N)=CC=2)CC1.Br[CH:23]([CH:41]([CH3:43])[CH3:42])[C:24]([O:26]CC1C=CC=C(OC2C=CC=CC=2)C=1)=[O:25]>>[CH2:1]([C:5]1[CH:6]=[CH:7][C:8]([NH:9][C@H:23]([C:24]([OH:26])=[O:25])[CH:41]([CH3:43])[CH3:42])=[CH:10][CH:11]=1)[CH2:2][CH2:3][CH3:4]

参加物

反応物 3

HCID 76944-Butylaniline

HCID 122539274-Cyclopropylaniline

HCID 13229492m-Phenoxybenzyl alpha-bromoisovalerate

生成物 1

HCID 53704978HCID 53704978、化合物

実験手順

Following the procedure of Example 1, each of 4-n-butylaniline and 4-cyclopropylaniline is reacted with m-phenoxybenzyl α-bromoisovalerate to yield the m-phenoxybenzyl ester of N-(4-n-butylphenyl)valine, MS m/e 431.2 (M+), and the m-phenoxybenzyl ester of N-(4-cyclopropylphenyl)valine, MS m/e 415.1 (M+).

出典と根拠

ORDレコード: ord-ffdc381163b84ffa9e789932aa55e01d
出典データセット: uspto-grants-1983_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04411912

反応ノート

読み込み中…

参加物