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Vanillin → N-benzyloxycarbony-D-valine isopropylamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Vanillin | HCID 1183 | — |
| 反応物 | Isopropylamine | HCID 6363 | — |
| 反応物 | N-alpha-Benzyloxycarbonyl-D-valine | HCID 712434 | — |
| 溶媒 | Ethyl acetate hexane | HCID 21226206 | — |
| 生成物 | N-benzyloxycarbony-D-valine isopropylamide | HCID 14723623 | — |
反応手順
Reaction of N-benzyloxycarbonyl-D-valine with isopropylamine by the method of Example 20, Part A afforded a quantitative yield of N-benzyloxycarbonyl-D-valine isopropylamide of Rf 0.61 (TLC, ethyl acetate/hexane, 1:1, vanillin spray).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04411925 |
| 出典データセット | uspto-grants-1983_10 |
| ORD ID | ord-a78262aeb3914eefbefc37a1791946a5 |
| 出典メモ | uspto-grants-1983_10 |