化工社化工社 化学情報印刷レポート · 研究参考用
Triethylamine → 3-Vinyldimethylsilyl-2-oxazolidinone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | 2-Oxazolidinone | HCID 73949 | — |
| 反応物 | Chloro(dimethyl)vinylsilane | HCID 519368 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | 3-Vinyldimethylsilyl-2-oxazolidinone | HCID 131715486 | — |
反応手順
A 3-vinyldimethylsilyl-2-oxazolidinone was prepared in accordance with the following procedure. A mixture of 34.8 grams of 2-oxazolidinone and 48.17 grams of vinyldimethylchlorosilane was prepared in 750 ml of tetrahydrofuran solvent. 40.26 grams of triethylamine was added dropwise. The mixture was then heated in a distillation apparatus with continuous reflux for a period of 30 minutes.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04736046 |
| 出典データセット | uspto-grants-1988_04 |
| ORD ID | ord-b469417e4ceb4c9baeefa2b560fdf6e7 |
| 出典メモ | uspto-grants-1988_04 |