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Lactic Acid → 2-(p-Nonylphenoxy)ethanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Lactic Acid | HCID 612 | — |
| 反応物 | 4-Nonylphenol | HCID 1752 | — |
| 反応物 | Ethylene Oxide | HCID 6354 | — |
| 触媒 | 4-Nonylphenol | HCID 1752 | — |
| 触媒 | Sodium Hydroxide | HCID 14798 | — |
| 生成物 | 2-(p-Nonylphenoxy)ethanol | HCID 7700 | — |
反応手順
In a stainless steel reactor having an inner volume of 1,000 ml and provided with a thermometer, a pressure gauge, and a stirrer, 200 g of nonylphenol (molecular weight 221), 0.6 g of sodium hydroxide as a catalyst, and 400 g of ethylene oxide were heated at 150° C. under pressure of 6.0 kg/cm2G of reaction. The resultant averagely 10-mole ethylene oxide adduct of nonylphenol and 2.7 g of an aqueous 50 wt% lactic acid solution added thereto were thoroughly stirred. The nonylphenol ethoxylate obtained as the result was tested for the effect of aging. The results are shown in Table 27.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04737314 |
| 出典データセット | uspto-grants-1988_04 |
| ORD ID | ord-3d510db927d24f7fbb54cd0c2a49e814 |
| 出典メモ | uspto-grants-1988_04 |