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HRID 648895作成日:2026年10月26日

Hydrazinecarboxaldehyde, 2-(4-nitrophenyl)- → Hydrazinecarboxaldehyde, 2-(4-aminophenyl)-

https://huagongshe.com/reaction/648895

反応式

関与物質

役割名称HCID仕込み量
反応物Hydrazinecarboxaldehyde, 2-(4-nitrophenyl)-HCID 5008489—
触媒HCID 178418390HCID 178418390—
溶媒EthanolHCID 702—
生成物Hydrazinecarboxaldehyde, 2-(4-aminophenyl)-HCID 11318981.9%

反応手順

Then, 30 g of 1-formyl-2-(4-nitrophenyl)hydrazine was catalytically reduced in 1.6 liters of ethanol at room temperature using palladium-carbon as a catalyst. The reaction mixture was filtered to remove the catalyst and the filtrate was evaporated to dryness to provide 20.5 g of 1-formyl-2-(4-aminophenyl)hydrazine having a melting point of 123°-125° C. as a light brown solid.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04737452
出典データセットuspto-grants-1988_04
ORD IDord-7d946c2d603649f39489bd0293d466a3
出典メモuspto-grants-1988_04