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Piperidine → 1-[4-(4-Pyridinylamino)benzoyl]piperidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Piperidine | HCID 8082 | — |
| 反応物 | 4-(4-Pyridinylamino)benzoic acid | HCID 12896000 | — |
| 生成物 | 1-[4-(4-Pyridinylamino)benzoyl]piperidine | HCID 13712474 | 49.5% |
反応手順
1-[4-(4-Pyridinylamino)benzoyl]piperidine was prepared from 4-(4-pyridinylamino)benzoic acid and piperidine according to a procedure analogous to that of Example 48(b), and was obtained in 49.5% yield in the form of a buff powder, m.p. 170°-172° C. when recrystallized from acetonitrile.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04610991 |
| 出典データセット | uspto-grants-1986_09 |
| ORD ID | ord-64b455ccc0f942d6b583e9d13b6e7b4d |
| 出典メモ | uspto-grants-1986_09 |