Ethyl formate → 2-(N-Formyl-2-amino-ethyl)-furan

反応式

[NH2:1][CH2:2][CH2:3][C:4]1[O:5][CH:6]=[CH:7][CH:8]=1.[CH:9](OCC)=[O:10]>>[CH:9]([NH:1][CH2:2][CH2:3][C:4]1[O:5][CH:6]=[CH:7][CH:8]=1)=[O:10]

参加物

反応物 2

HCID 8025Ethyl formate

HCID 11328632-(Furan-2-yl)ethan-1-amine

生成物 1

HCID 137469342-(N-Formyl-2-amino-ethyl)-furan

実験手順

Here, 2-(2-amino-ethyl)furan (10.0 g, 0.090 mol) is refluxed with ethyl formate (80 ml, 1.0 mol) for 12 hours. The reaction product is concentrated by evaporation and distilled in vacuo.

後処理

concentrationThe reaction product is concentrated by evaporation
distillationdistilled in vacuo

出典と根拠

ORDレコード: ord-c39f5eca83bd43319f039e3f8864241f
出典データセット: uspto-grants-1988_04
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04737495

反応ノート

読み込み中…