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N-bromobutanimide → 2-(2,2-Dichlorovinyl)-benzyl bromide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-bromobutanimide | HCID 67184 | — |
| 反応物 | 2-(2,2-Dichlorovinyl)-toluene | HCID 13713127 | — |
| 溶媒 | 1,1,1-Trichloroethane | HCID 6278 | — |
| 生成物 | 2-(2,2-Dichlorovinyl)-benzyl bromide | HCID 13713128 | — |
反応手順
211 g (1.13 moles) of 2-(2,2-dichlorovinyl)-toluene, 251 g (1.41 moles) of N-bromosuccinimide and 2 g of azoisobutyronitrile in 1300 ml of dry 1,1,1-trichloroethane are refluxed, an additional 1 g of azoisobutyronitrile is added to the reaction mixture after one hour, and heating is continued for a further hour.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04611010 |
| 出典データセット | uspto-grants-1986_09 |
| ORD ID | ord-760ebf0ea2264cd3a5e2e56550388425 |
| 出典メモ | uspto-grants-1986_09 |