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2-Methylpyridine → 2-(2,2-Dichlorovinyl)-benzyl 2-(4-chlorophenyl)-isovalerate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methylpyridine | HCID 7975 | — |
| 反応物 | 2-(4-Chlorophenyl)-3-methylbutanoyl chloride | HCID 4178001 | — |
| 反応物 | 2-(2,2-Dichlorovinyl)-benzaldehyde | HCID 13713131 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 2-(2,2-Dichlorovinyl)-benzyl 2-(4-chlorophenyl)-isovalerate | HCID 13713135 | — |
反応手順
2.8 g (0.012 mole) of 2-(4-chlorophenyl)-isovaleryl chloride in 50 ml of absolute toluene are introduced into 1.2 g (0.013 mole) of -picoline and 3.2 g (0.015 mole) of 2-(2,2-dichlorovinyl)-benzaldehyde in a conical flask at room temperature, while stirring. After 30 minutes, the mixture is filtered under suction over silica gel, and washing is carried out with toluene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04611010 |
| 出典データセット | uspto-grants-1986_09 |
| ORD ID | ord-0f238b4ef3e5448f8833fd83cb856d4f |
| 出典メモ | uspto-grants-1986_09 |