化工社化工社 化学情報印刷レポート · 研究参考用
Benzaldehyde → alpha,alpha-Bis(3,5-di-tert-butyl-4-hydroxyphenylthio)toluene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzaldehyde | HCID 240 | — |
| 反応物 | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | alpha,alpha-Bis(3,5-di-tert-butyl-4-hydroxyphenylthio)toluene | HCID 13710010 | 66.3% |
反応手順
The procedure of Example 1 is repeated using 23.84 grams of 2,6-di-tert-butyl-4-mercaptophenol, 5.31 grams of benzaldehyde, and 150 ml of methyl alcohol. The product is triturated with methyl alcohol to give 18.74 grams (66% yield) of white crystals, mp 122°-124° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04611023 |
| 出典データセット | uspto-grants-1986_09 |
| ORD ID | ord-b62ff9936c7f41b984ee1d508e7d4ac6 |
| 出典メモ | uspto-grants-1986_09 |