Methanol → HCID 13710011、化合物

HRID 64940

反応式

HRID 64940 の反応式
[C:1]([C:5]1[CH:10]=[C:9]([SH:11])[CH:8]=[C:7]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:6]=1[OH:16])([CH3:4])([CH3:3])[CH3:2].[CH2:17]([CH:19]([CH2:22][CH2:23][CH2:24][CH3:25])[CH:20]=O)[CH3:18].[CH3:26][OH:27]>>[C:1]([C:5]1[CH:10]=[C:9]([S:11][CH:20]([S:11][C:9]2[CH:8]=[C:7]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:6]([OH:16])=[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[CH:10]=2)[CH:19]([CH2:17][CH3:18])[CH2:22][CH2:23][CH2:24][CH3:25])[CH:8]=[C:7]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:26]=1[OH:27])([CH3:4])([CH3:3])[CH3:2]

参加物

4

反応物 3

HCID 887MethanolHCID 312412-EthylhexanalHCID 703702,6-Di-tert-butyl-4-mercaptophenol

生成物 1

HCID 13710011HCID 13710011、化合物

実験手順

The procedure of Example 1 is repeated using 23.84 grams of 2,6-di-tert-butyl-4-mercaptophenol, 6.41 grams of 2-ethylhexanal, and 150 ml of methyl alcohol. The product is purified by dry-column chromatography to give 10.29 grams of a clear syrup.

後処理

  1. customThe product is purified by dry-column chromatography

出典と根拠

ORDレコード
ord-6fd87e6b59f448079a43bff64df13065
出典データセット
uspto-grants-1986_09
特許番号
US04611023

関連ノート

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