Methanol → 1,1-Bis(3,5-di-tert-butyl-4-hydroxyphenylthio)-2-ethylhexane
反応式
[C:1]([C:5]1[CH:10]=[C:9]([SH:11])[CH:8]=[C:7]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:6]=1[OH:16])([CH3:4])([CH3:3])[CH3:2].[CH2:17]([CH:19]([CH2:22][CH2:23][CH2:24][CH3:25])[CH:20]=O)[CH3:18].[CH3:26][OH:27]>>[C:1]([C:5]1[CH:10]=[C:9]([S:11][CH:20]([S:11][C:9]2[CH:8]=[C:7]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:6]([OH:16])=[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[CH:10]=2)[CH:19]([CH2:17][CH3:18])[CH2:22][CH2:23][CH2:24][CH3:25])[CH:8]=[C:7]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:26]=1[OH:27])([CH3:4])([CH3:3])[CH3:2]参加物
4
実験手順
The procedure of Example 1 is repeated using 23.84 grams of 2,6-di-tert-butyl-4-mercaptophenol, 6.41 grams of 2-ethylhexanal, and 150 ml of methyl alcohol. The product is purified by dry-column chromatography to give 10.29 grams of a clear syrup.
後処理
- customThe product is purified by dry-column chromatography