化工社化工社 化学情報印刷レポート · 研究参考用
Dimethyloctylamine → HCID 178419187、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethyloctylamine | HCID 16224 | — |
| 反応物 | borane;N,N-diethylethanamine | HCID 264094 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | HCID 178419187 | HCID 178419187 | 89% |
反応手順
Octyldimethylamine (20.4 grams; 0.130 mole) was heated with triethylamine borane (1.9 grams; 0.130 mole) at reflux temperature until 12.8 grams (98%) of triethylamine had been collected in a cold trap. The reaction residue was distilled at reduced pressure to give N-octyl-N,N-dimethylamine borane boiling at 98°-100° C./0.9 mm. Hg. (19.6 grams; 89% yield).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04740504 |
| 出典データセット | uspto-grants-1988_04 |
| ORD ID | ord-d602c547b2d447c5a70a59f83b9251c5 |
| 出典メモ | uspto-grants-1988_04 |