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Aniline → 6-Isopropyl-o-toluidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | O-Toluidine | HCID 7242 | — |
| 反応物 | Propylene | HCID 8252 | — |
| 生成物 | 6-Isopropyl-o-toluidine | HCID 78920 | — |
反応手順
2-Methyl-6-isopropyl aniline was prepared by the method of Example 2 using an H-Y zeolite catalyst for the condensation of aniline and propylene. The ortho-toluidine and propylene were fed to the reactor in a 1:5 molar ratio and at an LHSV of 0.25 based on o-toluidine. The reaction was conducted at 250° C. and 861 psig. The effluent product stream was analyzed by gas chromatography. Conversion of o-toluidine was 81.5%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04740620 |
| 出典データセット | uspto-grants-1988_04 |
| ORD ID | ord-ee4902f425e34214aaeafb0b03e5c094 |
| 出典メモ | uspto-grants-1988_04 |