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Hydrochloric Acid → HCID 21713540、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | 1,1,2,3,3-Pentamethylindan | HCID 14549 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 1H-Indene, octahydro-1,1,2,3,3-pentamethyl- | HCID 118537 | — |
| 生成物 | HCID 21713540 | HCID 21713540 | — |
反応手順
prepared according to the disclosure of U.S. Pat. No. 4,902,840 issued on Feb. 20, 1990, the specification for which is incorporated herein by reference; 20% 1,1,2,3,3-pentamethylindane and 35% hexahydro-1,1,2,3,3-pentamethylindane is heated to 150° C. Hydrogen chloride gas evolves and is passed through a caustic soda scrubber. This solution is then washed with a 5% aqueous sodium hydroxide solution, dried over anhydrous magnesium sulfate and used without further purification in the next step, the carrying out of an oxo-reaction.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06271193B1 |
| 出典データセット | uspto-grants-2001_08 |
| ORD ID | ord-0c5e48e985044412bfd33fa090a3cb16 |
| 出典メモ | uspto-grants-2001_08 |