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HRID 649739作成日:2026年10月24日

Hydrochloric Acid → HCID 21713540、化合物

https://huagongshe.com/ja/reaction/649739

反応式

関与物質

役割名称HCID仕込み量
反応物Hydrochloric AcidHCID 313—
反応物1,1,2,3,3-PentamethylindanHCID 14549—
反応物Sodium HydroxideHCID 14798—
反応物1H-Indene, octahydro-1,1,2,3,3-pentamethyl-HCID 118537—
生成物HCID 21713540HCID 21713540—

反応手順

prepared according to the disclosure of U.S. Pat. No. 4,902,840 issued on Feb. 20, 1990, the specification for which is incorporated herein by reference; 20% 1,1,2,3,3-pentamethylindane and 35% hexahydro-1,1,2,3,3-pentamethylindane is heated to 150° C. Hydrogen chloride gas evolves and is passed through a caustic soda scrubber. This solution is then washed with a 5% aqueous sodium hydroxide solution, dried over anhydrous magnesium sulfate and used without further purification in the next step, the carrying out of an oxo-reaction.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06271193B1
出典データセットuspto-grants-2001_08
ORD IDord-0c5e48e985044412bfd33fa090a3cb16
出典メモuspto-grants-2001_08