Hydrochloric Acid → HCID 21713540、化合物

HRID 649739

反応式

HRID 649739 の反応式
[CH3:1][C:2]1([CH3:14])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[C:4]([CH3:12])([CH3:11])[CH:3]1[CH3:13].[CH3:15]C1(C)C2C(CCCC2)C(C)(C)C1C.Cl.[OH-:30].[Na+]>>[CH3:11][C:4]1([CH3:12])[C:5]2[CH2:6][CH2:7][CH2:8][CH:9]([CH:15]=[O:30])[C:10]=2[C:2]([CH3:14])([CH3:1])[CH:3]1[CH3:13]

参加物

5

反応物 4

HCID 313Hydrochloric AcidHCID 145491,1,2,3,3-PentamethylindanHCID 14798Sodium HydroxideHCID 1185371H-Indene, octahydro-1,1,2,3,3-pentamethyl-

生成物 1

HCID 21713540HCID 21713540、化合物

実験手順

prepared according to the disclosure of U.S. Pat. No. 4,902,840 issued on Feb. 20, 1990, the specification for which is incorporated herein by reference; 20% 1,1,2,3,3-pentamethylindane and 35% hexahydro-1,1,2,3,3-pentamethylindane is heated to 150° C. Hydrogen chloride gas evolves and is passed through a caustic soda scrubber. This solution is then washed with a 5% aqueous sodium hydroxide solution, dried over anhydrous magnesium sulfate and used without further purification in the next step, the carrying out of an oxo-reaction.

後処理

  1. customprepared
  2. washThis solution is then washed with a 5% aqueous sodium hydroxide solution
  3. dry with materialdried over anhydrous magnesium sulfate
  4. customused without further purification in the next step
  5. customthe carrying out of an oxo-reaction

出典と根拠

ORDレコード
ord-0c5e48e985044412bfd33fa090a3cb16
出典データセット
uspto-grants-2001_08
特許番号
US06271193B1

関連ノート

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