化工社化工社 化学情報印刷レポート · 研究参考用
Lilial → HCID 11012960、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Lilial | HCID 228987 | — |
| 反応物 | Sodium cyanoborohydride | HCID 5003444 | — |
| 反応物 | 5-(Aminomethyl)-2-chloropyridine | HCID 7020927 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | HCID 11012960 | HCID 11012960 | — |
反応手順
Route A: After suspending 620 mg (9.84 mmol) of sodium cyanoborohydride in 2 ml of absolute methanol, 700 mg (4.91 mmol) of 6-chloro-3-pyridylmethylamine was added thereto. Subsequently, to this was added a solution of 1.0 g (4.90 mmol) 3-(4-t-butylphenyl)-2-methylpropionaldehyde/2 ml absolute methanol by portions and then, stirring was conducted at room temperature for 4 h.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06271385B1 |
| 出典データセット | uspto-grants-2001_08 |
| ORD ID | ord-6b8c0a22c7ca4e8ea28cefd9cd3dcabd |
| 出典メモ | uspto-grants-2001_08 |