化工社化工社 化学情報印刷レポート · 研究参考用
Catechol → Guaiacol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Catechol | HCID 289 | — |
| 反応物 | Methanol | HCID 887 | — |
| 生成物 | Guaiacol | HCID 460 | — |
| 生成物 | Phenol | HCID 996 | — |
反応手順
When the temperature of the catalyst stratum reached 260° C. in Example 43 and 300° C. in Example 44, a starting compound mixture consisting of catechol and methyl alcohol in a mixing molar ratio of 1:3.44 was evaporated in an evaporator, and the resultant starting compound mixture gas was fed in a feeding rate of 10.5 g/min. together with a nitrogen gas into the reaction tube for 14 hours, to etherify catechol with methyl alcohol and to produce a dihydric phenol compound monoalkylether, i.e., guaiacol. The reaction mixture gas discharged from the reaction tube was cooled to a temperature of 40° C. The resultant liquefied product was collected from the reaction mixture.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05248835 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-bc1049bbac104ae6857eeaa65fae9134 |
| 出典メモ | uspto-grants-1993_09 |