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HRID 6505作成日:2026年10月24日

Catechol → Guaiacol

https://huagongshe.com/ja/reaction/6505

反応式

関与物質

役割名称HCID仕込み量
反応物CatecholHCID 289—
反応物MethanolHCID 887—
生成物GuaiacolHCID 460—
生成物PhenolHCID 996—

反応手順

When the temperature of the catalyst stratum reached 260° C. in Example 43 and 300° C. in Example 44, a starting compound mixture consisting of catechol and methyl alcohol in a mixing molar ratio of 1:3.44 was evaporated in an evaporator, and the resultant starting compound mixture gas was fed in a feeding rate of 10.5 g/min. together with a nitrogen gas into the reaction tube for 14 hours, to etherify catechol with methyl alcohol and to produce a dihydric phenol compound monoalkylether, i.e., guaiacol. The reaction mixture gas discharged from the reaction tube was cooled to a temperature of 40° C. The resultant liquefied product was collected from the reaction mixture.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05248835
出典データセットuspto-grants-1993_09
ORD IDord-bc1049bbac104ae6857eeaa65fae9134
出典メモuspto-grants-1993_09