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Hydrochloric Acid → 9-(1,3-di-n-octanoyloxy-2 propoxymethyl)guanine HCl
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Diethyl Ether | HCID 3283 | — |
| 反応物 | 9-(1,3-Di-n-octanoyloxy-2-propoxymethyl)guanine | HCID 136332159 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 9-(1,3-di-n-octanoyloxy-2 propoxymethyl)guanine HCl | HCID 136332160 | — |
反応手順
A twofold stoichiometric excess of 3% hydrogen chloride in methanol is added to a solution of 1.0 g. of 9-(1,3-di-n-octanoyloxy-2-propoxymethyl)guanine in 20 ml methanol. Diethyl ether is added until precipitation is complete. The product is filtered, washed with ether, air dried and recrystallized to give 9-(1,3-di-n-octanoyloxy-2-propoxymethyl)guanine hydrochloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04612314 |
| 出典データセット | uspto-grants-1986_09 |
| ORD ID | ord-44085480c8624b88860ea735b0070417 |
| 出典メモ | uspto-grants-1986_09 |