関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Benzoyl chloride | HCID 7412 | — |
| 反応物 | Carbonic acid, di-2-propen-1-yl ester | HCID 84764 | — |
| 生成物 | Allyl benzoate | HCID 11406 | 90% |
反応手順
The following example illustrates the use of basic amine catalysts. A mixture of benzoyl chloride (7.03 g, 0.05 mole), diallyl carbonate (7.10 g, 0.05 mole) and N,N-dimethylaminopyridine (0.06 g) were combined in a glass reaction vessel and heated to 170° C. for 4 hours. Distillation of the reaction mixture gave allyl benzoate, b.p. 110° C.-111° C. (13 mm Hg). Yield was 90 percent.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US04612386 |
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| 出典データセット | uspto-grants-1986_09 |
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| ORD ID | ord-c28c4553598f4116b96b8136652ed85e |
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| 出典メモ | uspto-grants-1986_09 |
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