Phosphoric Acid → Phosphate cerium nitrate

HRID 651417

反応式

HRID 651417 の反応式
O.O.O=[Al]O[Si](O[Si](O[Al]=O)=O)=O.[P:14](=[O:18])([OH:17])([OH:16])[OH:15].[N+:19]([O-:22])([O-:21])=[O:20].[Ce+3:23].[N+]([O-])([O-])=O.[N+]([O-])([O-])=O.[C:32]([O-:37])(=[O:36])[C:33]([O-:35])=[O:34].[V+5:38].[C:39]([O-:44])(=[O:43])[C:40]([O-:42])=[O:41].[C:45]([O-:50])(=[O:49])[C:46]([O-:48])=[O:47].[C:51]([O-:56])(=[O:55])[C:52]([O-:54])=[O:53].[C:57]([O-:62])(=[O:61])[C:58]([O-:60])=[O:59].[V+5]>O>[P:14]([O-:18])([O-:17])([O-:16])=[O:15].[N+:19]([O-:22])([O-:21])=[O:20].[Ce+3:23].[N+:19]([O-:22])([O-:21])=[O:20].[N+:19]([O-:22])([O-:21])=[O:20].[C:32]([O-:37])(=[O:36])[C:33]([O-:35])=[O:34].[V+5:38].[C:39]([O-:44])(=[O:43])[C:40]([O-:42])=[O:41].[C:45]([O-:50])(=[O:49])[C:46]([O-:48])=[O:47].[C:51]([O-:56])(=[O:55])[C:52]([O-:54])=[O:53].[C:57]([O-:62])(=[O:61])[C:58]([O-:60])=[O:59].[V+5:38]

参加物

7

反応物 4

HCID 1004Phosphoric AcidHCID 24948Cerium nitrateHCID 56841936BentoneHCID 178526029HCID 178526029、化合物

生成物 2

HCID 86755301Phosphate cerium nitrateHCID 178526029HCID 178526029、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

A clay/phosphate/cerium nitrate, vanadium oxalate slurry was prepared by adding 1340 grams of Theile RC-320 kaolin clay slurry to 1795 milliliters of water in a high speed mixer. To this mixture, 192 grams of phosphoric acid was added. Thereafter, 431 grams of cerium nitrate solution and 232 grams of vanadium oxalate solution were added to the slurry. The slurry was then spray dried and then resulting particles were calcined at 650° C. for 30 minutes in a muffle furnace. The calcined particles were then mixed with magnesium oxide in a 50/50 weight percent ratio and analyzed by TGA tests. These tests indicated that the resulting material produced an SOx absorption of 0.27% per minute.

後処理

  1. customThe slurry was then spray dried
  2. additionThe calcined particles were then mixed with magnesium oxide in a 50/50 weight percent ratio
  3. customproduced
  4. customan SOx absorption of 0.27% per minute

出典と根拠

ORDレコード
ord-977f05274d54448da420464fdee03879
出典データセット
uspto-grants-2001_08
特許番号
US06281164B1

関連ノート

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