化工社化工社 化学情報印刷レポート · 研究参考用
Potassium Carbonate → Sotalol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | Sotalol Hydrochloride | HCID 66245 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Sotalol | HCID 5253 | — |
反応手順
In 2 lit. round bottom flask, in 450 ml of water, (±) sotalol hydrochloride (200 g) was added under stirring at room temperature. Under stirring, a solution of 500 g of potassium carbonate in 300 ml of water was added. The stirring was continued for 48 hours. Solid material was separated to give 107 g of (±) sotalol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06281246B1 |
| 出典データセット | uspto-grants-2001_08 |
| ORD ID | ord-83949e398a5643a2bda1cdc453c2439c |
| 出典メモ | uspto-grants-2001_08 |