化工社化工社 化学情報印刷レポート · 研究参考用
6-Chlorobenzo[b]thiophene-2-sulfonyl chloride → 6-Chloro-benzo[b]thiophene-2-sulfonic acid (2-oxo-1-prop-2-ynyl-pyrrolidin-3-(s)-yl)amide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 6-Chlorobenzo[b]thiophene-2-sulfonyl chloride | HCID 15158641 | — |
| 反応物 | 3-(S)-amino-1-prop-2-ynyl-pyrrolidin-2-one hydrochloride | HCID 20680730 | — |
| 生成物 | 6-Chloro-benzo[b]thiophene-2-sulfonic acid (2-oxo-1-prop-2-ynyl-pyrrolidin-3-(s)-yl)amide | HCID 53892522 | — |
反応手順
The title compound is prepared as described in EXAMPLE 1, Part K using 6-chloro-benzo[b]thiophene-2-sulfonyl chloride and 3-(S)-amino-1-prop-2-ynyl-pyrrolidin-2-one hydrochloride as starting material. The crude product is isolated as a beige foam and used in the subsequent step without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06281227B1 |
| 出典データセット | uspto-grants-2001_08 |
| ORD ID | ord-05187c3376004192a615c0c17db4dc1e |
| 出典メモ | uspto-grants-2001_08 |