化工社化工社 化学情報印刷レポート · 研究参考用
2-Methylimidazole hydrochloride → Triphenyl-(4-vinyl)phenylboron 2-methylimidazolium
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methylimidazole hydrochloride | HCID 521629 | — |
| 反応物 | Triphenyl-(4-vinyl)phenylboron sodium | HCID 131714859 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | Triphenyl-(4-vinyl)phenylboron 2-methylimidazolium | HCID 131714857 | 94% |
反応手順
Triphenyl-(4-vinyl)phenylboron sodium (0.05 moles) was reacted with 2-methylimidazole hydrochloride (0.05 moles) in the similar manner to that of Example 4 using acetone as the reaction solvent to give 20.0 g (yield: 93.7%) of the titled compound as colorless crystal. M.p. 234° to 236° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04613373 |
| 出典データセット | uspto-grants-1986_09 |
| ORD ID | ord-fa0c064ca8c44442a9f38018331b1a91 |
| 出典メモ | uspto-grants-1986_09 |