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1-(3-Bromopropoxy)-3-nitrobenzene → 3-(3-Bromopropoxy)-aniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(3-Bromopropoxy)-3-nitrobenzene | HCID 7172301 | — |
| 触媒 | Nickel | HCID 935 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | 3-(3-Bromopropoxy)-aniline | HCID 459256 | — |
反応手順
1 g of Raney nickel is added to a solution of 4 g of 3-(3-bromopropoxy)-nitrobenzene in 40 ml of tetrahydrofuran and the starting substance is hydrogenated at room temperature. The catalyst is filtered off and washed with tetrahydrofuran. Evaporation of the filtrate gives 3-(3-bromopropoxy)-aniline as a colourless oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04670604 |
| 出典データセット | uspto-grants-1987_06 |
| ORD ID | ord-0bc7908018df4e4c82b06dbd11cc14b4 |
| 出典メモ | uspto-grants-1987_06 |