Lauroyl peroxide → Acetic acid ethenyl ester, polymer with 2,5-furandione

HRID 652392

反応式

HRID 652392 の反応式
[C:1]([O:4][CH:5]=[CH2:6])(=[O:3])[CH3:2].[C:7]1(=[O:13])[O:12][C:10](=[O:11])[CH:9]=[CH:8]1.C(OOC(=O)CCCCCCCCCCC)(=O)CCCCCCCCCCC>C1C=CC=CC=1>[C:1]([O:4][CH:5]=[CH2:6])(=[O:3])[CH3:2].[C:10]1(=[O:11])[O:12][C:7](=[O:13])[CH:8]=[CH:9]1

参加物

5

反応条件

温度
70 °C

実験手順

13 g (0.5 mole) of vinyl acetate, 49 g (0.5 mole) of maleic acid anhydride and 0.1 g of lauroyl peroxide were dissolved in 400 cc of benzene and heated for five hours at 70° C. The copolymer was precipitated from the viscous solution with petroleum ether (80° to 100° C.). The copolymer dissolved well in diluted caustic soda.

後処理

  1. customThe copolymer was precipitated from the viscous solution with petroleum ether (80° to 100° C.)
  2. dissolutionThe copolymer dissolved well in diluted caustic soda

出典と根拠

ORDレコード
ord-a8ca235c9ca844d4bdd9af51edf5e228
出典データセット
uspto-grants-1987_06
特許番号
US04671982

関連ノート

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