関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Glycol monoethyl ether | HCID 8076 | — |
| 反応物 | Nickel Acetate | HCID 9756 | — |
| 反応物 | N-Methylanthranilic acid | HCID 67069 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | N-methylanthranilic acid nickel | HCID 86741584 | 138.2% |
反応手順
23.8 g (0.1 mol) of nickel acetate was added to 500 ml of ethyl cellosolve and stirred. The mixture was heated to 50° C., and 30.2 g (0.2 mol) of N-methyl-anthranilic acid was gradually added. The mixture was subjected to reaction for 2 hours at about 130° C. under refluxing and then dispersed in 2 liters of water. After 1 hour, the dispersion was subjected to filtration and the precipitate was washed with water until neutrality. The precipitate was then dried at 90° C. to obtain about 29 g of pale blue powder.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04673631 |
|---|
| 出典データセット | uspto-grants-1987_06 |
|---|
| ORD ID | ord-12a820d4ef814cc28280da2d675a0e64 |
|---|
| 出典メモ | uspto-grants-1987_06 |
|---|
