Aniline → HCID 18931494、化合物

反応式

[N+:1]([C:4]1[C:5]([N+:13]([O-:15])=[O:14])=[C:6]([CH:10]=[CH:11][CH:12]=1)[C:7](Cl)=[O:8])([O-:3])=[O:2].[NH2:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[N+:1]([C:4]1[C:5]([N+:13]([O-:15])=[O:14])=[C:6]([CH:10]=[CH:11][CH:12]=1)[C:7]([NH:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)=[O:8])([O-:3])=[O:2]

参加物

反応物 2

HCID 6115Aniline

HCID 11413586Dinitrobenzoyl chloride

生成物 1

HCID 18931494HCID 18931494、化合物

実験手順

Dinitrobenzoyl chloride is caused to react with aniline so as to give dinitrobenzanilide. Thereafter, the resulting product is caused to react with Ar--N(R)2 and oxyphosphorous chloride and to the resulting product concentrated hydrochloric acid is added to prepare a compound having the formula: ##STR5##

出典と根拠

ORDレコード: ord-fd2a7a569840467c836697f1a1801e28
出典データセット: uspto-grants-1987_06
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04673773

反応ノート

読み込み中…