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5-Amino-2-methylphenol → Indoaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Amino-2-methylphenol | HCID 17818 | — |
| 反応物 | 2,5-Dimethoxy benzoquinone diimine | HCID 53963286 | — |
| 溶媒 | Ammonia | HCID 222 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Indoaniline | HCID 24748760 | 3.2% |
反応手順
0.02 mole (0.246 g) 3-amino-6-methyl phenol is dissolved in 30 cc water to which 5 cc ammonia 22° Be were added. To this solution there is added 0.02 mole (0.332 g) 2,5-dimethoxy benzoquinone diimine from the first stage in solution in 60 cc water. The mixture is agitated for 20 minutes. Thereafter the reaction mixture is filtered off, yielding 0.125 g of said indoaniline which exhibits a melting point of 104°.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04675130 |
| 出典データセット | uspto-grants-1987_06 |
| ORD ID | ord-10fb56145be74612acdb95b2510182ed |
| 出典メモ | uspto-grants-1987_06 |