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Dipotassium tetrachloroplatinate → Platinous chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dipotassium tetrachloroplatinate | HCID 61440 | — |
| 反応物 | Sodium Acetate | HCID 517045 | — |
| 反応物 | 1,1-Bis(aminomethyl)cyclobutane dihydrochloride | HCID 20203628 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Platinous chloride | HCID 2770 | — |
| 生成物 | 1,1-Cyclobutanedimethanamine | HCID 432836 | — |
反応手順
A solution of 1.87 g of the above amine in 30 ml of water was treated with 1.64 g of solid sodium acetate followed by 4.15 g of potassium tetrachloroplatinate. The mixture was stirred overnight and filtered. The filtrate was concentrated, giving as a solid 1,1-cyclobutanedimethanamine, compound with platinum chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04675336 |
| 出典データセット | uspto-grants-1987_06 |
| ORD ID | ord-e8ec9817642b46d08a31487737b3a61d |
| 出典メモ | uspto-grants-1987_06 |