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3-Methyl-3-buten-1-ol → 3-Methyl-3-butenyl 2-methylisocrotonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Methyl-3-buten-1-ol | HCID 12988 | — |
| 反応物 | Methyl (2Z)-2-methyl-2-butenoate | HCID 5356352 | — |
| 反応物 | Dioctyltin laurate | HCID 22292224 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 3-Methyl-3-butenyl 2-methylisocrotonate | HCID 16205381 | — |
反応手順
A mixture of 20.0 g. of methyl angelate, 22.65 g. of 3-methyl-3-butenyl alcohol, 100 ml. of toluene and 0.8 g. of dioctyltin laurate was reacted under the same conditions as in Example 6. The reaction mixture was subjected to single distillation to obtain 39.5 g. of a distillate boiling at 104° C. (32 mmHg).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04613680 |
| 出典データセット | uspto-grants-1986_09 |
| ORD ID | ord-af7ccfea57244031a639864f8090c451 |
| 出典メモ | uspto-grants-1986_09 |