化工社化工社 化学情報印刷レポート · 研究参考用
3-Hexenol → 2-Butenoic acid, 2-methyl-, (3Z)-3-hexenyl ester, (2Z)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Hexenol | HCID 5281167 | — |
| 反応物 | Methyl (2Z)-2-methyl-2-butenoate | HCID 5356352 | — |
| 反応物 | Dioctyltin laurate | HCID 22292224 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 2-Butenoic acid, 2-methyl-, (3Z)-3-hexenyl ester, (2Z)- | HCID 16220109 | — |
反応手順
A mixture of 20.0 g. of methyl angelate, 26.34 g. of (Z)-3-hexenyl alcohol, 100 ml. of toluene and 1.2 g. of dioctyltin laurate was placed in a 300 ml. glass flask, which was equipped with a Soxhlet extractor filled on the top with molecular sieve 4A and a reflux cooler.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04613680 |
| 出典データセット | uspto-grants-1986_09 |
| ORD ID | ord-86d99ad2c96d423794886a4f3cc76510 |
| 出典メモ | uspto-grants-1986_09 |