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Sodium Hydroxide → Acifluorfen sodium
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Acifluorfen | HCID 44073 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Acifluorfen sodium | HCID 44072 | 105.4% |
反応手順
5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (1.7 g, 0.0047 mole) is dissolved in methanol (25 ml) and sodium hydroxide (4.7 ml of 1N NaOH in methanol, 0.0047 mole) is added rapidly. The solvent is then removed in vacuo to give 1.9 g of product that decomposes at 217° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04613360 |
| 出典データセット | uspto-grants-1986_09 |
| ORD ID | ord-9e9b4f013e6e41fe8d4ab299c0212c3e |
| 出典メモ | uspto-grants-1986_09 |