化工社化工社 化学情報印刷レポート · 研究参考用
Heptane → Toluene heptane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Heptane | HCID 8900 | — |
| 反応物 | 2,4-Dibromophenol | HCID 12005 | — |
| 反応物 | Phenol, 2,4-dibromo-, phosphate (3:1) | HCID 14670658 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Toluene heptane | HCID 22263336 | — |
反応手順
Two hundred and eighty-four grams of crude tris-(2,4-dibromophenyl)phosphate were mixed with 808 grams of a solution of 85% n-heptane and 15% toluene as above. The liquid portion weighed 733 grams and contained 0.047% 2,4-dibromophenol, 1.45% ester product and 0.06% chloridates.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05128496 |
| 出典データセット | uspto-grants-1992_07 |
| ORD ID | ord-555e4b438369405a8d9ce68fee2899ca |
| 出典メモ | uspto-grants-1992_07 |