Hydrochloric Acid → Ethyl 3,5-dimethyl-4-hydroxybenzoate

HRID 654215

反応式

HRID 654215 の反応式
[OH:1][C:2]1[C:10]([CH3:11])=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][C:3]=1[CH3:12].[CH2:13](O)[CH3:14].Cl>O>[OH:1][C:2]1[C:3]([CH3:12])=[CH:4][C:5]([C:6]([O:8][CH2:13][CH3:14])=[O:7])=[CH:9][C:10]=1[CH3:11]

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 702EthanolHCID 1383874-Hydroxy-3,5-dimethylbenzoic acid

生成物 1

HCID 3027494Ethyl 3,5-dimethyl-4-hydroxybenzoate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

A mixture of 500 mg (3 mmol) of 4-hydroxy-3,5-dimethylbenzoic acid, 20 ml of absolute ethanol and a catalytic amount of anhydrous HCl was heated at reflux for 2 h. The mixture was then poured into excess cold water and the resultant precipitate was filtered. The precipitate was washed with water and dried in-vacuo to give the title compound as a white solid.

後処理

  1. temperatureat reflux for 2 h
  2. filtrationthe resultant precipitate was filtered
  3. washThe precipitate was washed with water
  4. customdried in-vacuo

出典と根拠

ORDレコード
ord-494493c611f549bcb599c2de434f9249
出典データセット
uspto-grants-1992_07
特許番号
US05130335

関連ノート

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