HCID 18962537、化合物 → 5-methoxy-1H-indol-4-ol

反応式

C([O:8][C:9]1[C:17]([O:18][CH2:19]C)=[CH:16][CH:15]=[C:14]2[C:10]=1[CH:11]=[CH:12][NH:13]2)C1C=CC=CC=1.C(OC1C(OC)=CC=C2C=1C=CN2)C1C=CC=CC=1>>[OH:8][C:9]1[C:17]([O:18][CH3:19])=[CH:16][CH:15]=[C:14]2[C:10]=1[CH:11]=[CH:12][NH:13]2

参加物

反応物 2

HCID 18962537HCID 18962537、化合物

HCID 18962543HCID 18962543、化合物

生成物 1

HCID 158384075-methoxy-1H-indol-4-ol収率 90%

実験手順

This compound is obtained according to the operating method described in Example 1d, in which the 4-benzyloxy-5-ethoxyindole is replaced with 4-benzyloxy-5-methoxyindole. A white powder (yield=90%, m.p.=146° C., decomposition) is obtained.

後処理

customThis compound is obtained
customA white powder (yield=90%, m.p.=146° C., decomposition) is obtained

出典と根拠

ORDレコード: ord-81d3cf6a273d4ab78adc12fced93f8d0
出典データセット: uspto-grants-1992_07
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05131911

反応ノート

読み込み中…

参加物