反応式
[CH:1]1[CH:6]=[CH:5][C:4]([N:7]=[C:8](Cl)Cl)=[CH:3][CH:2]=1.C(N(CC)CC)C.[OH:18][CH2:19][CH:20]1[CH2:25][CH2:24][CH2:23][CH2:22][NH:21]1>C(Cl)Cl>[C:4]1([N:7]=[C:8]2[N:21]3[CH2:22][CH2:23][CH2:24][CH2:25][CH:20]3[CH2:19][O:18]2)[CH:5]=[CH:6][CH:1]=[CH:2][CH:3]=1参加物
5
実験手順
3 g Phenyl isocyanide dichloride in 10 ml methylene chloride was treated at room temperature with a solution of 5.4 ml triethylamine and 1.7 g 2-hydroxymethylpiperidine in 20 ml methylene chloride. After 12 hours at room temperature, the mixture was washed with water, the organic phase was dried over magnesium sulphate, the solvent was distilled and the residue recrystallised from diisopropyl ether.
後処理
- washthe mixture was washed with water
- dry with materialthe organic phase was dried over magnesium sulphate
- distillationthe solvent was distilled
- customthe residue recrystallised from diisopropyl ether
出典と根拠
- ORDレコード
- ord-783c1be8ceb944d8b2390e4b3079cd9b
- 出典データセット
- uspto-grants-1992_07
- 特許番号
- US05131946
関連ノート
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