化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hypochlorite → Sodium 3,3-dimethyl-2-oxobutyrate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hypochlorite | HCID 23665760 | — |
| 反応物 | Sodium 3,3-dimethyl-2-hydroxybutyrate | HCID 23694960 | — |
| 触媒 | Ruthenium dioxide hydrate | HCID 16211523 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Sodium 3,3-dimethyl-2-oxobutyrate | HCID 23674764 | — |
反応手順
Sodium 3,3-dimethyl-2-hydroxybutyrate and ruthenium dioxide hydrate are added to water, the pH rendered alkaline, and sodium hypochlorite is slowly added to produce sodium 3,3-dimethyl-2-oxobutyrate in high yield and purity. The solid catalyst is filtered off and may be re-used while the filtrate can be directly used in further synthesis.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04614822 |
| 出典データセット | uspto-grants-1986_09 |
| ORD ID | ord-0abcb0c150bc4175a08041240e6ed897 |
| 出典メモ | uspto-grants-1986_09 |