化工社化工社 化学情報印刷レポート · 研究参考用
5-(1-Naphthyl)-4-pentyn-1-ol → 5-(Naphth-1-yl)pentanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-(1-Naphthyl)-4-pentyn-1-ol | HCID 19955557 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | 5-(Naphth-1-yl)pentanol | HCID 10353200 | — |
反応手順
A mixture of 5-(1-naphthyl)-4-pentyn-1-ol (500 ng, 2.37 mmol) and 5% palladium on barium sulfate (5 mg) in ethyl ether (30 ml) was stirred at room temperature under a hydrogen atmosphere for two days. Solvent removal, after filtration through celite, gave the title compound as a yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05134128 |
| 出典データセット | uspto-grants-1992_07 |
| ORD ID | ord-fc1489072aa34dfd8d39a00b9d7dfcbb |
| 出典メモ | uspto-grants-1992_07 |