化工社化工社 化学情報印刷レポート · 研究参考用
Diethylmethylamine → Methanesulfonic acid, 1,1,1-trifluoro-, compd. with N-ethyl-N-methylethanamine (1:1)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diethylmethylamine | HCID 12022 | — |
| 反応物 | Trifluoromethanesulfonic acid | HCID 62406 | — |
| 生成物 | Methanesulfonic acid, 1,1,1-trifluoro-, compd. with N-ethyl-N-methylethanamine (1:1) | HCID 86620365 | — |
反応手順
Equimolar amounts of diethylmethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed diethylmethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08071253B2 |
| 出典データセット | uspto-grants-2011_12 |
| ORD ID | ord-9f5289c08f2941199dbef871e4dcb7eb |
| 出典メモ | uspto-grants-2011_12 |