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HRID 655343作成日：2026年10月26日

5-Methyloxazolo[4,5-b]pyridin-2(3H)-one → 5-methyl-3-[3-(5-methylpyridin-2-yl)benzyl]-3H-oxazolo[4,5-b]-pyridin-2-one

https://huagongshe.com/reaction/655343

反応式

関与物質

役割名称HCID仕込み量
反応物5-Methyloxazolo[4,5-b]pyridin-2(3H)-oneHCID 10012075—
反応物(3-(5-Methylpyridin-2-yl)phenyl)methanolHCID 56604357—
生成物5-methyl-3-[3-(5-methylpyridin-2-yl)benzyl]-3H-oxazolo[4,5-b]-pyridin-2-oneHCID 59564723—

反応手順

Reaction of [3-(5-methylpyridin-2-yl)phenyl]methanol with 5-methyl-3H-oxazolo[4,5-b]pyridin-2-one under Mitsunobu conditions gives the desired 5-methyl-3-[3-(5-methylpyridin-2-yl)benzyl]-3H-oxazolo[4,5-b]-pyridin-2-one, ESI 332 (M+H).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08071593B2
出典データセットuspto-grants-2011_12
ORD IDord-322d0eb93d354295b175707aa24d076f
出典メモuspto-grants-2011_12