化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Benzenediazonium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Benzenamine hydrochloride (1:1) | HCID 8870 | — |
| 反応物 | Sodium Nitrite | HCID 23668193 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Benzenediazonium chloride | HCID 60992 | — |
反応手順
A solution of benzenediazonium chloride was prepared as follows: To an ice cold (about 5° C.) solution of aniline hydrochloride (3.24 g., 25 mmoles) in water (10 ml.) and concentrated hydrochloric acid (2.1 ml., 25 mmoles) was added dropwise with stirring a solution of sodium nitrite (1.9 g., 27.5 mmoles) in water (10 ml.). After addition the solution was stirred in the cold for an additional 15 minutes.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04128425 |
| 出典データセット | uspto-grants-1978_12 |
| ORD ID | ord-9a32150a3bf545fe94a430c25ee8ca32 |
| 出典メモ | uspto-grants-1978_12 |