関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-Methylbenzenesulfonic acid | HCID 6925 | — |
| 反応物 | Sodium Carbonate | HCID 10340 | — |
| 反応物 | 2-Methyl-1-pentene | HCID 12986 | — |
| 反応物 | 4-Mercaptophenol | HCID 240147 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 4-(Hexylthio)phenol | HCID 20086310 | — |
反応手順
A 4-(hexylthio)phenol was prepared as follows. In a one liter flask equipped with thermometer, stirring rod and water condenser was added 126 grams of 4-mercaptophenol and 7 grams of toluenesulfonic acid. The flask contents were heated to 60° C. and 93 grams of 2-methyl-1-pentene were added over a fifty minute period. The flask contents were neutralized with 9 grams of Na2CO3 in aqueous solution and decanted. The reaction product was stripped to a pot temperature of 80° C. at 20 millimeters of mercury. It weighed 216 grams.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04128530 |
|---|
| 出典データセット | uspto-grants-1978_12 |
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| ORD ID | ord-ab70397f3e6949cf95fb20215605e801 |
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| 出典メモ | uspto-grants-1978_12 |
|---|
