関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | N-Phenylphthalimide | HCID 68215 | — |
| 反応物 | Maleic Acid | HCID 444266 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Phthalic Anhydride | HCID 6811 | — |
| 生成物 | N-Phenylmaleimide | HCID 13662 | — |
反応手順
A mixture of 2.32 parts of maleic acid, 2.23 parts of N-phenyl phthalimide and 20 parts of water is heated under sealed conditions for 2 hours at 180° C. The reaction mixture is then allowed to cool to ambient conditions and distilled under vacuum. Maleic anhydride is initially recovered followed by phthalic anhydride and N-phtnyl maleimide. There is obtained a yield of 16% by weight of phthalic anhydride and 14.1% by weight of N-phenylmaleimide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04128574 |
|---|
| 出典データセット | uspto-grants-1978_12 |
|---|
| ORD ID | ord-d29f888cbcaa45d6800b090bb8a32222 |
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| 出典メモ | uspto-grants-1978_12 |
|---|
