化工社化工社 化学情報印刷レポート · 研究参考用
2-Methylcyclohexanone → Methyl 3-(1-methyl-2-oxocyclohexyl)propanoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methylcyclohexanone | HCID 11419 | — |
| 反応物 | 2-Methylcyclopentanone | HCID 14265 | — |
| 反応物 | 1-Methyl-2-oxocyclopentanepropionic acid methyl ester | HCID 12291889 | — |
| 生成物 | Methyl 3-(1-methyl-2-oxocyclohexyl)propanoate | HCID 574325 | — |
反応手順
In the same manner but replacing 2-methylcyclohexanone with an equivalent amount of 2-methylcyclopentanone, 1-methyl-2-oxocyclopentanepropionic acid methyl ester, bp 88°-100° C./1.1 mm, nmr (CDCl3) δ 1.0 (s, 3H), 1.8 (m, 6H), 2.3 (m, 4H), 3.7 (s, 3H), is obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04128560 |
| 出典データセット | uspto-grants-1978_12 |
| ORD ID | ord-0ac5163d69744a34a58712d9781fbae8 |
| 出典メモ | uspto-grants-1978_12 |