Propylenediamine → HCID 178442710、化合物

関与物質

反応条件

反応手順

1,2-Diaminopropane 61.5 g (0.7 mole) was delivered to a reaction vessel and pelargonic acid 112 g (0.7 mole) was added slowly. The mixture was slowly heated to 170° C. while removing water of reaction. There was obtained 4-methyl-2-octyl-2-imidazoline. To it was added 42 g of paraformaldehyde with stirring. The mixture was heated to about 100° C. for 3 hours to produce N1 -hydroxymethyl-4-methyl-2-octyl-2-imidazoline.

情報源と証拠