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Acetic Acid → 4-Chloro-1-naphthol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Hydrogen Bromide | HCID 260 | — |
| 反応物 | 1-Chloro-4-methoxynaphthalene | HCID 606038 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 4-Chloro-1-naphthol | HCID 11787 | — |
反応手順
The known compound 1-chloro-4-methoxynaphthalene is dissolved in 150 ml. of acetic acid and 150 ml. of 48 percent hydrobromic acid, and the mixture is heated at its reflux temperature for 2 hours. The mixture is diluted with 200 ml. of water and cooled to provide 1-chloro-4-hydroxynaphthalene as a crystalline solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04128659 |
| 出典データセット | uspto-grants-1978_12 |
| ORD ID | ord-03d39e03caed4569923ddc9bb0d2b986 |
| 出典メモ | uspto-grants-1978_12 |