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Hydrochloric Acid → 2-Chloro-3-fluoroaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 2-Chloro-1-fluoro-3-nitrobenzene | HCID 88883 | — |
| 生成物 | 2-Chloro-3-fluoroaniline | HCID 88884 | — |
反応手順
19.6 g. of 2-chloro-3-fluoronitrobenzene (0.11 mole) is reduced with stannous chloride (118 g., 0.63 mole) in 180 ml. of concentrated hydrochloric acid. The solution is basified with aqueous sodium hydroxide and extracted with chloroform to yield 2-chloro-3-fluoroaniline.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04128666 |
| 出典データセット | uspto-grants-1978_12 |
| ORD ID | ord-1db00a5a9136416fb08e3a530f59cd2f |
| 出典メモ | uspto-grants-1978_12 |