Orotic Acid → Creatine orotate
反応式
O.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:10])[NH2:9])[CH3:7])[OH:4].[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1>C(O)C>[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4]参加物
4
実験手順
Under room temperature 149 grams of creatine monohydrate is slowly added to 1.5 liters of ethanol under agitation and stirring for 30 minutes. Then 156 grams of orotic acid is slowly added to the mixture during continuous stirring for 4 hours under room temperature. Finally filtration is utilized to remove the solvent and clean the residue with ethanol. After drying 272 grams of creatine orotate is obtained.
後処理
- stirringduring continuous stirring for 4 hours under room temperature
- filtrationFinally filtration
- customto remove the solvent
- dry with materialAfter drying 272 grams of creatine orotate
- customis obtained
出典と根拠
- ORDレコード
- ord-90a9bcc616464073b559974dbcdb47a5
- 出典データセット
- uspto-grants-2011_12
- 特許番号
- USRE043029E1
反応ノート
読み込み中…