Orotic Acid → Dicreatine orotate
反応式
O.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:10])[NH2:9])[CH3:7])[OH:4].[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1>C(O)C>[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4].[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4]参加物
4
実験手順
Under room temperature 298 grams of creatine monohydrate is slowly added to 2.5 liters of ethanol under agitation and stirring for 30 minutes. Then 156 grams of orotic acid is slowly added to the mixture during continuous stirring for 4 hours under room temperature. Finally filtration is utilized to remove the solvent and clean the residue with ethanol. After drying 410 grams of Dicreatine orotate is obtained.
後処理
- stirringduring continuous stirring for 4 hours under room temperature