Orotic Acid → Tricreatine orotate

HRID 657441

反応式

HRID 657441 の反応式
O.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:10])[NH2:9])[CH3:7])[OH:4].[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1>C(O)C>[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4].[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4].[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4]

参加物

4

反応物 2

HCID 967Orotic AcidHCID 80116Creatine Monohydrate

生成物 1

HCID 11444210Tricreatine orotate

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

Under room temperature 447 grams of creatine monohydrate is slowly added to 3.5 liters of ethanol under agitation and stirring for 30 minutes. Then 156 grams of orotic acid is slowly added to the mixture during continuous stirring for 4 hours under room temperature. Finally filtration is utilized to remove the solvent and clean the residue with alcohol. After drying 555 grams of Tricreatine orotate is obtained.

後処理

  1. stirringduring continuous stirring for 4 hours under room temperature
  2. filtrationFinally filtration
  3. customto remove the solvent
  4. dry with materialAfter drying 555 grams of Tricreatine orotate
  5. customis obtained

出典と根拠

ORDレコード
ord-9e2a2e1f8b6146c28c4ae7c7957b50e8
出典データセット
uspto-grants-2011_12
特許番号
USRE043029E1

関連ノート

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